| Bruker SMART APEXII area-detector diffractometer | 3330 reflections with I > 2σ(I) |
| ω and φ scans | Rint = 0.021 |
| Absorption correction: multi-scan (SADABS; Bruker, 2008) | θmax = 29.2°, θmin = 2.8° |
| Tmin = 0.752, Tmax = 0.863 | h = −32→24 |
| 10728 measured reflections | k = −40→24 |
| 5181 independent reflections | l = −12→12 |