| Stoe IPDS 2 diffractometer | 2726 independent reflections |
| Radiation source: sealed X-ray tube, 12 x 0.4 mm long-fine focus | 1196 reflections with I > 2σ(I) |
| Plane graphite monochromator | Rint = 0.103 |
| Detector resolution: 6.67 pixels mm-1 | θmax = 25.0°, θmin = 1.9° |
| rotation method scans | h = −6→6 |
| Absorption correction: integration (X-RED32; Stoe & Cie, 2002) | k = −14→14 |
| Tmin = 0.844, Tmax = 0.973 | l = −25→25 |
| 8675 measured reflections |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.