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. Author manuscript; available in PMC: 2020 Mar 20.
Published in final edited form as: J Pharm Biomed Anal. 2018 Dec 19;166:105–112. doi: 10.1016/j.jpba.2018.12.028

Table 7:

Results of HPLC Assays (mg of oxytocin per vial)

Sample No Lab 1 Lab 2 Lab 8 Lab 11 Lab 12 Lab 13 Lab 14
1 1.829 1.851 1.777 1.801 1.825 1.720 1.822
2 1.808 1.861 1.785 1.822 1.816 1.740 1.830
3 1.819 1.852 1.777 1.815 1.815 1.706 1.806
4 1.818 1.910 1.793 1.798 1.815 1.734 1.829
5 1.827 1.861 1.781 1.819 1.845 1.726 1.827
6 1.830 1.857 1.786 1.823 1.823 1.737 1.820
7 1.816 1.843 1.787 1.819 1.818 1.721 1.820
8 1.810 1.859 1.785 1.822 1.794 1.747 1.822

Statistical analysis indicated that the result of 1.910 mg by Lab 2 was an outlier. With this exclusion, the sample mean was 1.806. The lab-to-lab variance (reproducibility) and the sample-to-sample variance within each lab (repeatability) are summarized in Table 8.