Fig 3. Products of CYP6DJ1 assays with terpinolene and products detected in female beetles after treatment with terpinolene.

Four unidentified terpinolene-derived metabolites are present in extracts of terpinolene treated beetles (peaks 11–14), three of which, (peaks 12–14) are found in CYP6DJ1 assays with terpinolene. Chromatograms are shown with the total of the extracted ions 91, 94, 108, 109, 119, 121, 137, 152 m/z. Retention indices and mass spectra of peaks 1–10 are shown in S2 Table and S6 Fig.