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(a) Cyclic voltammogram for [i-PrNDI]Ni2(CPh2) (3) (0.4 M [nBu4N][PF6] supporting electrolyte in THF, glassy carbon working electrode, 100 mV/s scan rate). The open circuit potential and direction of the scan is indicated by an arrow. (b) Synthesis and (c) solid-state structure of [K(18-Crown-6)(THF)2][(i-PrNDI)Ni2(CPh2) (4). [K(18-Crown-6)(THF)2] is omitted for clarity. Ni1–Ni2: 2.3816(9) Å.
