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. 2019 Mar 26;75(Pt 4):499–505. doi: 10.1107/S2056989019003694
Cl1—C12 1.745 (3) Cl1'—Cl1'i 2.275 (9)
C12—C13 1.389 (4) C12'—C13' 1.389 (17)
C12—C11 1.397 (5) C12'—C11' 1.399 (18)
C11—C10 1.371 (4) C11'—C10' 1.368 (19)
C11—H11 0.9500 C11'—H11' 0.9500
C10—C9 1.398 (4) C10'—C9' 1.391 (17)
C10—H10 0.9500 C10'—H10' 0.9500
C9—C14 1.407 (4) C9'—C14' 1.388 (15)
C9—C8 1.462 (4) C9'—C8' 1.467 (15)
C14—C13 1.382 (4) C14'—C13' 1.383 (16)
C14—H14 0.9500 C14'—H14' 0.9500
C13—H13 0.9500 C13'—H13' 0.9500
C8—C7 1.344 (3) C8'—C7' 1.331 (14)
C8—H8 0.9500 C8'—H8' 0.9500
C7—C15 1.442 (3) C7'—C15' 1.448 (14)
C7—C1 1.483 (4) C7'—C1' 1.483 (15)
C15—N2 1.146 (5) C15'—N2' 1.148 (17)
C1—C6 1.402 (4) C1'—C6' 1.377 (16)
C1—C2 1.402 (4) C1'—C2' 1.410 (18)
C2—C3 1.382 (5) C2'—C3' 1.40 (2)
C2—H2 0.9500 C2'—H2' 0.9500
C3—C4 1.393 (5) C3'—C4' 1.41 (2)
C3—H3 0.9500 C3'—H3' 0.9500
C4—C5 1.390 (4) C4'—C5' 1.376 (17)
C4—H4 0.9500 C4'—H4' 0.9500
C5—C6 1.384 (4) C5'—C6' 1.369 (16)
C5—H5 0.9500 C5'—H5' 0.9500
C6—H6 0.9500 C6'—H6' 0.9500
Cl1'—C12' 1.735 (15)
C13—C12—C11 121.7 (3) C13'—C12'—C11' 122.6 (16)
C13—C12—Cl1 118.7 (2) C13'—C12'—Cl1' 118.0 (14)
C11—C12—Cl1 119.6 (3) C11'—C12'—Cl1' 119.1 (15)
C10—C11—C12 118.1 (4) C10'—C11'—C12' 118 (2)
C10—C11—H11 120.9 C10'—C11'—H11' 120.8
C12—C11—H11 120.9 C12'—C11'—H11' 120.8
C11—C10—C9 122.1 (3) C11'—C10'—C9' 121.2 (19)
C11—C10—H10 119.0 C11'—C10'—H10' 119.4
C9—C10—H10 119.0 C9'—C10'—H10' 119.4
C10—C9—C14 118.2 (3) C14'—C9'—C10' 118.6 (14)
C10—C9—C8 117.6 (2) C14'—C9'—C8' 122.3 (14)
C14—C9—C8 124.2 (2) C10'—C9'—C8' 119.1 (15)
C13—C14—C9 120.7 (2) C13'—C14'—C9' 122.5 (15)
C13—C14—H14 119.6 C13'—C14'—H14' 118.8
C9—C14—H14 119.6 C9'—C14'—H14' 118.8
C14—C13—C12 119.0 (2) C14'—C13'—C12' 116.7 (15)
C14—C13—H13 120.5 C14'—C13'—H13' 121.6
C12—C13—H13 120.5 C12'—C13'—H13' 121.6
C7—C8—C9 129.4 (2) C7'—C8'—C9' 130.8 (14)
C7—C8—H8 115.3 C7'—C8'—H8' 114.6
C9—C8—H8 115.3 C9'—C8'—H8' 114.6
C8—C7—C15 120.9 (2) C8'—C7'—C15' 120.8 (13)
C8—C7—C1 124.3 (2) C8'—C7'—C1' 124.7 (12)
C15—C7—C1 114.7 (2) C15'—C7'—C1' 114.4 (13)
N2—C15—C7 177.6 (5) N2'—C15'—C7' 173 (5)
C6—C1—C2 118.2 (3) C6'—C1'—C2' 114.6 (15)
C6—C1—C7 120.6 (3) C6'—C1'—C7' 123.4 (15)
C2—C1—C7 121.1 (3) C2'—C1'—C7' 121.9 (16)
C3—C2—C1 120.7 (3) C3'—C2'—C1' 119 (2)
C3—C2—H2 119.7 C3'—C2'—H2' 120.4
C1—C2—H2 119.7 C1'—C2'—H2' 120.4
C2—C3—C4 120.8 (4) C2'—C3'—C4' 123 (2)
C2—C3—H3 119.6 C2'—C3'—H3' 118.6
C4—C3—H3 119.6 C4'—C3'—H3' 118.6
C5—C4—C3 118.9 (3) C5'—C4'—C3' 115.1 (18)
C5—C4—H4 120.6 C5'—C4'—H4' 122.5
C3—C4—H4 120.6 C3'—C4'—H4' 122.5
C6—C5—C4 120.8 (3) C6'—C5'—C4' 120.5 (17)
C6—C5—H5 119.6 C6'—C5'—H5' 119.8
C4—C5—H5 119.6 C4'—C5'—H5' 119.8
C5—C6—C1 120.6 (3) C5'—C6'—C1' 125.6 (17)
C5—C6—H6 119.7 C5'—C6'—H6' 117.2
C1—C6—H6 119.7 C1'—C6'—H6' 117.2
C12'—Cl1'—Cl1'i 122.6 (7)
C13—C12—C11—C10 −4.3 (8) Cl1'i—Cl1'—C12'—C11' −142.8 (8)
Cl1—C12—C11—C10 177.0 (4) C13'—C12'—C11'—C10' −0.02 (15)
C12—C11—C10—C9 1.2 (9) Cl1'—C12'—C11'—C10' 174.0 (14)
C11—C10—C9—C14 2.3 (7) C12'—C11'—C10'—C9' 0.02 (15)
C11—C10—C9—C8 −179.1 (5) C11'—C10'—C9'—C14' −0.1 (3)
C10—C9—C14—C13 −2.9 (4) C11'—C10'—C9'—C8' 178.7 (14)
C8—C9—C14—C13 178.7 (3) C10'—C9'—C14'—C13' 0.1 (5)
C9—C14—C13—C12 −0.1 (4) C8'—C9'—C14'—C13' −178.6 (15)
C11—C12—C13—C14 3.8 (6) C9'—C14'—C13'—C12' −0.1 (4)
Cl1—C12—C13—C14 −177.5 (2) C11'—C12'—C13'—C14' 0.1 (3)
C10—C9—C8—C7 152.5 (3) Cl1'—C12'—C13'—C14' −174.0 (14)
C14—C9—C8—C7 −29.0 (5) C14'—C9'—C8'—C7' −31 (3)
C9—C8—C7—C15 −0.2 (4) C10'—C9'—C8'—C7' 150.5 (17)
C9—C8—C7—C1 −176.9 (2) C9'—C8'—C7'—C15' −1 (3)
C8—C7—C1—C6 154.5 (3) C9'—C8'—C7'—C1' 178.5 (17)
C15—C7—C1—C6 −22.4 (3) C8'—C7'—C1'—C6' 155 (2)
C8—C7—C1—C2 −25.4 (4) C15'—C7'—C1'—C6' −25 (3)
C15—C7—C1—C2 157.7 (3) C8'—C7'—C1'—C2' −29 (3)
C6—C1—C2—C3 −0.5 (4) C15'—C7'—C1'—C2' 151 (2)
C7—C1—C2—C3 179.5 (3) C6'—C1'—C2'—C3' 8 (5)
C1—C2—C3—C4 0.5 (4) C7'—C1'—C2'—C3' −168 (4)
C2—C3—C4—C5 −0.7 (4) C1'—C2'—C3'—C4' −18 (8)
C3—C4—C5—C6 0.9 (4) C2'—C3'—C4'—C5' 13 (7)
C4—C5—C6—C1 −0.9 (4) C3'—C4'—C5'—C6' 1 (5)
C2—C1—C6—C5 0.6 (4) C4'—C5'—C6'—C1' −10 (4)
C7—C1—C6—C5 −179.3 (2) C2'—C1'—C6'—C5' 5 (4)
Cl1'i—Cl1'—C12'—C13' 31.4 (14) C7'—C1'—C6'—C5' −178 (2)