Table 3. Experimental details.

Crystal data
Chemical formula	C22H22O
M r	302.39
Crystal system, space group	Monoclinic, P21/n
Temperature (K)	150
a, b, c (Å)	9.8037 (9), 8.9815 (9), 18.8946 (17)
β (°)	90.985 (4)
V (Å3)	1663.5 (3)
Z	4
Radiation type	Mo Kα
μ (mm−1)	0.07
Crystal size (mm)	0.52 × 0.28 × 0.06
Data collection
Diffractometer	Bruker D8 VENTURE
Absorption correction	Multi-scan (SADABS; Bruker, 2014 ▸)
T min, T max	0.735, 0.996
No. of measured, independent and observed [I > 2σ(I)] reflections	15325, 3808, 2471
R int	0.115
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S	0.070, 0.171, 1.12
No. of reflections	3808
No. of parameters	211
H-atom treatment	H-atom parameters constrained
Δρmax, Δρmin (e Å−3)	0.30, −0.26

Computer programs: APEX3 (Bruker, 2015 ▸), SAINT (Bruker, 2014 ▸), SHELXT (Sheldrick, 2015a ▸), SHELXL2014 (Sheldrick, 2015b ▸), ORTEP-3 for Windows (Farrugia, 2012 ▸), DIAMOND (Brandenburg & Berndt, 2001 ▸) and CRYSCALc (T. Roisnel, local program, version of 2015).