Table 3. Substrate scope of dehydrogenation of aliphatic alcohols ^a .

^a0.2 mmol alcohol, 1 mol% Ptpop-BF₂-IV, under N₂, CD₃CN (1 mL) in an NMR tube, 365 nm LED irradiation, 8 hours. Yield determined by ¹H NMR spectroscopy. For dehydrogenation of benzyl alcohols, the reactions were stopped after complete consumption of substrates.