Table 5. One-pot cascade synthesis of quinazolin-4(3H)-ones a .
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a0.4 mmol alcohol, 0.2 mmol anthranilamide, 2 mol% Ptpop-I, 5 mol% nBu4NCl, H2O/CH2Cl2 1 : 3 (3 mL), under N2, 410 nm LEDs irradiation, 8 hours; isolated yields.
bThe ethanol solution containing 0.2 mmol anthranilamide and 2 mol% Ptpop-BF2-IV was under N2 and 365 nm LEDs irradiation; isolated yield.