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. Author manuscript; available in PMC: 2020 Apr 1.
Published in final edited form as: J Biomol NMR. 2019 Feb 25;73(3-4):141–153. doi: 10.1007/s10858-019-00237-5

Figure 1:

Figure 1:

A. Pulse sequences for the conventional 2D Z-filtered TEDOR experiment. B. Hybrid pulse sequence (TEDOR-NCX) that combines TEDOR and NCA (or NCO) experiments. C. 1D spectrum of U-13C,15N SLN recorded using conventional TEDOR experiment (black). D. 1D TEDOR and NCA spectra of U-13C,15N SLN acquired simultaneously with the TEDOR-NCA pulse sequence (blue and red). The phase cycles were ϕ1=y, −y, y, −y. ϕ2=y, y, −y, −y, and ϕreceiver=y, −y, −y, y. XY-4 phase cycling scheme was applied for 15N π pulses during TEDOR mixing periods. States mode detection of t1 dimension was obtained by switching the ϕ* phase between y and −x.