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. 2019 May 6;2019:5459862. doi: 10.1155/2019/5459862

Table 1.

1H NMRa and 13C NMRb data of 1 in CD3OD (δ in ppm, J in Hz).

No. of H 1H NMRa No. of C 13C NMRb
1 1 130.3
2 7.14 (d, J = 8.5 Hz) 2 130.7
3 6.72 (d, J = 8.5 Hz) 3 116.0
4 4 158.2
5 6.72 (d, J = 8.5 Hz) 5 116.0
6 7.14 (d, J = 8.5 Hz) 6 130.7
7 4.45 (2H, s) 7 74.3
1′ 1′ 136.6
2′ 7.26 (d, J = 8.5 Hz) 2′ 129.4
3′ 7.08 (d, J = 8.5 Hz) 3′ 117.7
4′ 4′ 158.4
5′ 7.08 (d, J = 8.5 Hz) 5′ 117.7
6′ 7.26 (d, J = 8.5 Hz) 6′ 129.4
7′ 4.54 (2H, s) 7′ 64.8
1 4.88 (d, J = 7.0 Hz) 1 102.3
2 3.45 (m) 2 78
3 3.36 (m) 3 71.7
4 3.60 (m) 4 77.1
5 3.45 (m) 5 74.9
6a 3.60 (m) 6 70.4
6b 3.85 (d, J = 9.5 Hz)

a500 MHz, in CD3OD. b125 MHz in CD3OD.