Table 1.
No. of H | 1H NMRa | No. of C | 13C NMRb |
---|---|---|---|
1 | 1 | 130.3 | |
2 | 7.14 (d, J = 8.5 Hz) | 2 | 130.7 |
3 | 6.72 (d, J = 8.5 Hz) | 3 | 116.0 |
4 | 4 | 158.2 | |
5 | 6.72 (d, J = 8.5 Hz) | 5 | 116.0 |
6 | 7.14 (d, J = 8.5 Hz) | 6 | 130.7 |
7 | 4.45 (2H, s) | 7 | 74.3 |
1′ | 1′ | 136.6 | |
2′ | 7.26 (d, J = 8.5 Hz) | 2′ | 129.4 |
3′ | 7.08 (d, J = 8.5 Hz) | 3′ | 117.7 |
4′ | 4′ | 158.4 | |
5′ | 7.08 (d, J = 8.5 Hz) | 5′ | 117.7 |
6′ | 7.26 (d, J = 8.5 Hz) | 6′ | 129.4 |
7′ | 4.54 (2H, s) | 7′ | 64.8 |
1″ | 4.88 (d, J = 7.0 Hz) | 1″ | 102.3 |
2″ | 3.45 (m) | 2″ | 78 |
3″ | 3.36 (m) | 3″ | 71.7 |
4″ | 3.60 (m) | 4″ | 77.1 |
5″ | 3.45 (m) | 5″ | 74.9 |
6″a | 3.60 (m) | 6″ | 70.4 |
6″b | 3.85 (d, J = 9.5 Hz) |
a500 MHz, in CD3OD. b125 MHz in CD3OD.