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Variation of the nature of the base for the O-methylation of glycerol (1) in subcritical methanol.
 | ||
|---|---|---|
| Entry | Base (16 mol%) | Yield of 2 (%) |
| 1 | K2CO3 | 39 |
| 2 | CaCO3 | 0 |
| 3 | Na2CO3 | 8 |
| 4 | Cs2CO3 | 40 |
| 5 | (NH4)2CO3 | 0 |
| 6 | NaOH | 4 |
| 7 | KOH | 6 |
| 8 | K3PO4 | 4 |
| 9 | AcONa | 11 |
| 10 | DABCO | 0 |
| 11 | Ag2O | 0 |
| 12 | Na | 9 |
