Table 4.
Effect of water for the O-methylation of glycerol (1) in subcritical methanol.
 | |||
|---|---|---|---|
| Entry | Water (mL) | HC(OCH3)3 (mol%) | Yield of 2 (%) |
| 1 | – | 0 | 39 |
| 2 | anhydrous | 0 | 35 |
| 3 | 1 | 0 | 25 |
| 4 | – | 100 | 21 |
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