Table 5.
Scale down and scale up study for the O-methylation of glycerol (1) in subcritical methanol.
 | ||
|---|---|---|
| Entry | Methanol (mL) | Yield of 2 (%) |
| 1 | 20 | 29 |
| 2 | 50 | 30 |
| 3 | 70 | 39 |
| 4 | 350 | 35 |
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