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. Author manuscript; available in PMC: 2020 Jun 11.
Published in final edited form as: Angew Chem Int Ed Engl. 2019 May 8;58(24):8029–8033. doi: 10.1002/anie.201902489

Table 1.

Connection of iminosulfur oxydifluorides 1 and 1° amines 2.[a, b]

graphic file with name nihms-1025080-t0006.jpg
[a]

Reactions were performed with 1 (0.10 mmol), 2 (0.10 mmol), MeCN 50 mL, pH 7.3 aq. PBS buffer 50 mL, at 25 °C for 5 minutes unless otherwise stated.

[b]

Isolated yield.

[c]

For 3 d and 3 e, the reaction was carried out for 1 hour.