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. 2019 Jun 6;9:8351. doi: 10.1038/s41598-019-44806-y

Table 2.

Preparation conditions of kaolinite/methanol intercalation composite.

Method Precursor Precursor mass/g Temp./°C Time/h Total methanol dosage/mL Ref.
S.E. KD 5 65 8 100 This work
S.T. KD 10 200–230 35 30 21
S.T. KD 1 100 24 300 15
S.R. KNMF a. t. 168 26
S.R. KD 5 a. t. 240 1200 23
S.R. KD 20 a. t. 192 4040 18
S.R. KD 5 a. t. 168 100 19

S.E. = Soxhlet extraction; S.T. = Solvothermal; S.R. = Stirring; a.t. = ambient temperature.