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. 2019 May 23;2019:4851279. doi: 10.1155/2019/4851279

Table 1.

Identification of phenolic compounds in ethanol extract from leaves of C. scolymus using their retention times, LC/MS, and LC–MS/MS data.

Peaka RT (min) m/z Mode (+/-) ƛ max (min) MS/MS Tentative ID
1 3.00 122.3 + 200-700 82 Salicylic acid-o-hexoside
2 3.7 117.2 - 200-700 100 Chlorogenic acid
3 4.2 112 - 200-700 214.8, 178.8, 352.8 3-mono-o-cafeoylquinic acid
4 5.3 141 - 200-700 265.9 Apigenin-7-glucoside
5 8.4 223 - 200-700 331.4 Unknown
6 10.30 275 - 200-700 529.7, 350.8, 284.7 Luteolin-7-o-rutinoside
7 13.5 327.1 - 200-700 170.9 Dihydroxypropiophend-hexoside
8 14.8 395 - 200-700 529.7, 288. 9,307 Kampferol 3-o-rutinoside
9 16.2 431 - 200-700 434.7, 294.9, 344.8 Quercetin-o-pentoside
10 23.3 623 - 200-700 255.1 Caffeic acid

Identification was aided by comparison with reference standards that were available and by correlation with previous literature reports.

a Peak numbers and retention times (Rt) refer to LC/MS chromatograms in Figure 2.