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. Author manuscript; available in PMC: 2020 Jun 12.
Published in final edited form as: J Am Chem Soc. 2019 May 28;141(23):9106–9123. doi: 10.1021/jacs.9b03337

Scheme 8.

Scheme 8.

HIE with N,N-dimethylbenzamide catalyzed by (a) [Ir(COD)(pyridine)(PCy3)]PF6 (reference 61). Conditions: 23°C, CH2Cl2, 24 h. (b) (H4-iPrCNC)Fe(N2)2 (reference 61). Conditions: 45°C, THF, 24 h.