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. 2019 May 7;11(5):254. doi: 10.3390/toxins11050254

Table 2.

Validation data of mycotoxins from artificially contaminated beer samples.

Mycotoxin Spiking Level [ng/mL] Calculated Concentration [ng/mL] Recovery [%] Precision [%] LOD
[ng/mL]
LOQ
[ng/mL]
OTA 0.05 0.0408 81.6 2.5 0.003 0.011
0.25 0.199 79.6 6.1
1.0 0.858 85.8 4.2
DON 40 38.16 95.4 2.9 3.50 11.6
200 190.6 95.3 1.2
400 378.2 94.5 3.9
NIV 40 40.84 102.1 5.2 4.30 14.3
200 202.2 101.1 1.7
400 407.2 101.8 1.3
T-2 8 9.36 117.0 3.9 0.31 1.03
40 44.64 111.6 3.0
80 92.8 116.0 1.3
HT-2 8 9.10 113.8 5.2 0.36 1.21
40 47.64 119.1 3.0
80 93.04 116.3 1.2
DAS 8 8.72 109.0 4.0 0.28 0.92
40 43.92 109.8 2.6
80 84.64 105.8 4.1
ZEN 4 4.14 103.5 3.4 0.07 0.23
20 20.74 103.7 2.5
40 42.56 106.4 3.0