Table 2.
Mycotoxin | Spiking Level [ng/mL] | Calculated Concentration [ng/mL] | Recovery [%] | Precision [%] | LOD [ng/mL] |
LOQ [ng/mL] |
---|---|---|---|---|---|---|
OTA | 0.05 | 0.0408 | 81.6 | 2.5 | 0.003 | 0.011 |
0.25 | 0.199 | 79.6 | 6.1 | |||
1.0 | 0.858 | 85.8 | 4.2 | |||
DON | 40 | 38.16 | 95.4 | 2.9 | 3.50 | 11.6 |
200 | 190.6 | 95.3 | 1.2 | |||
400 | 378.2 | 94.5 | 3.9 | |||
NIV | 40 | 40.84 | 102.1 | 5.2 | 4.30 | 14.3 |
200 | 202.2 | 101.1 | 1.7 | |||
400 | 407.2 | 101.8 | 1.3 | |||
T-2 | 8 | 9.36 | 117.0 | 3.9 | 0.31 | 1.03 |
40 | 44.64 | 111.6 | 3.0 | |||
80 | 92.8 | 116.0 | 1.3 | |||
HT-2 | 8 | 9.10 | 113.8 | 5.2 | 0.36 | 1.21 |
40 | 47.64 | 119.1 | 3.0 | |||
80 | 93.04 | 116.3 | 1.2 | |||
DAS | 8 | 8.72 | 109.0 | 4.0 | 0.28 | 0.92 |
40 | 43.92 | 109.8 | 2.6 | |||
80 | 84.64 | 105.8 | 4.1 | |||
ZEN | 4 | 4.14 | 103.5 | 3.4 | 0.07 | 0.23 |
20 | 20.74 | 103.7 | 2.5 | |||
40 | 42.56 | 106.4 | 3.0 |