Table A6.

Overview of GC-MS methods in mycotoxins analysis.

Mycotoxin/ Metabolite	Matrix	Sample Pre-Treatment			GC-MS			Year of Publication	Reference
		Extraction	Clean-Up	Derivatization	Ionization/ Ion Selection	Scan Mode	LOD; LOQ (µg/kg) or (µg/L)
DON	Wheat; complete feed for pigs; complete farm-mixed wet feed for pigs	NM	NM	NM	NM	NM	NM; 10	2016	[165]
DON	Durum wheat	MeCN 82%	Charcoal/Alumina/Celite column	TMSIM-TMCS (100/1 v/v)	NM	SIM	0.01; NM	2016	[197]
3-AcDON
15-AcDON
T-2	Wheat; complete feed for pigs; complete farm-mixed wet feed for pigs	NM	NM	NM	NM	NM	NM; 10	2016	[165]
HT-2							NM; 10
T-2 + HT-2							NM; 10

NM—Not mentioned; TMSIM—trimethylsilylimidazole; TMCS—trimethylchlorosilane.