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a) Conversion (mol %) vs. time (min) for the dehydrocoupling of Me2NH⋅BH3 with 5 mol % (•) and 10 mol % (▪) of 1 in C6D6 at 60 °C. Data obtained by in situ monitoring of the reaction by 11B NMR. b) Graph tracking concentration of substrate (Me2NH⋅BH3), product ([Me2NBH2]2; 3), Me2N=BH2 (4), and Me2NH‐BH2‐NMe2‐BH3 (5) over reaction course. Concentrations determined by in situ 11B NMR measurements at 60 °C in C6D6. Initial concentrations [3]=0.29 m, [1]=15 mm.
