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Cyclic voltammograms of a 1.0 mM solution of 2 (red) under a nitrogen atmosphere and after addition of 5 eq. of TFAA (blue). The voltammograms are plotted versus the potential of a Ag/AgCl reference electrode in (n-Bu4N)(ClO4)/CH3CN at a scan rate of 100 mV/s using a Pt working electrode. MoV/ MoIV potentials: Protonated 2 −135 mV, non-protonated 2 −501 mV, vs Fc/Fc+.
