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. 2019 Jun 10;56(7):3264–3271. doi: 10.1007/s13197-019-03783-w

Fig. 3.

Fig. 3

Isothermal LF-NMR studies of wet and freeze-dried (FD) beads. Crystallization is displayed as a function of time at − 20 (a) − 30 (b) − 70 °C (c). Experimental values were fitted by the association single phase equation (at − 20 and − 30 °C) and the Avrami equation (− 70 °C)