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. 2019 May 31;61(3):138–146. doi: 10.5187/jast.2019.61.3.138

Table 1. Results for validation parameters (Dried pea).

Nicotinic acid Nicotinamide
Linear regression equation y = 371,678x − 106,410 y = 649,469x + 33,576
r2 0.9979 0.9978
Range of linearity (μg/mL) 1–10 1–10
Repeatability (RSD, n = 10) 2.0% 2.0%
Reproducibility (RSD of intra-day studies, n = 16) 2.08% 2.04%
LOD (μg/mL) 0.005 0.004
LOQ (μg/mL) 0.018 0.013
Accuracy (a, recovery; b, RSD; n = 10) 104.2%a, 0.34%b 96.4%a, 0.28%b

x, amount (μg/mL); y, peak area; r2, correlation coefficient;

LOD, limit of detection; LOQ, limit of quantification; RSD, relative standard deviation.