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. 2016 Dec 2;56(2):559–562. doi: 10.1002/anie.201610182

Figure 1.

Figure 1

Long‐term experiment. Reaction conditions: MeOH/H2O (20 mL, ratio 9:1), triglyme (20 mL), 8 m KOH, 1 (2.1 μmol, 0.05 mm), 10 equiv. PNPiPr ligand; T set: 92 °C.