Table 2.

Values of crystallinity index (CrI), hemicellulose percentage (%HC), lateral fibril dimensions (LFD) and lateral fibril aggregate dimensions (LFAD) and accessible/total fibril surface ratio (AS/(AS + IAS)), calculated from the C4-region deconvolution of the solid-state ¹³C CP/MAS NMR spectra from the starting bleached birchwood Kraft fibers (KF), PaLPMO9E-treated bleached birchwood Kraft fibers (KF-LPMO), Ultra Turrax dispersed PaLPMO9E-treated fibers (NFC0) and PaLPMO9E-treated fibers submitted to mechanical shearing (NFC1–3)

Sample	CrI (%)	HC (%)	LFDa (nm)	LFADa (nm)	AS/ (AS + IAS)
KF	50.28 ± 2.99	22.42 ± 2.39	2.27 ± 0.13	19.05 ± 4.43	24.18 ± 4.38
KF-LPMO	49.94 ± 1.54	18.97 ± 2.23	2.20 ± 0.07	18.00 ± 2.18	24.86 ± 2.29
NFC0	51.13 ± 0.93	19.12 ± 0.52	2.23 ± 0.93	15.14 ± 0.42	29.67 ± 0.42
NFC1	53.71 ± 0.02	19.82 ± 1.35	2.12 ± 0.06	14.69 ± 2.39	32.77 ± 2.39
NFC2	47.88 ± 0.02	18.85 ± 2.34	2.39 ± 0.12	11.29 ± 0.40	36.73 ± 0.40
NFC3	47.65 ± 0.80	20.19 ± 1.17	2.39 ± 0.03	9.33 ± 0.43	43.86 ± 0.43

^aAssuming a factor of 0.57 nm