Table 2.
DC, % | RPmax, %/s | PS, MPa | VS, % | FM, GPa | FS, MPa | |
---|---|---|---|---|---|---|
Resin | ||||||
One-way ANOVA, P value | <0.001 | <0.001 | <0.001 | <0.001 | 0.056 | 0.010 |
Control resin | 63.9 (0.4)a | 9.4 (0.2)a | 2.8 (0.1) a | 6.4 (0.5)a | 2.7 (0.2) | 121.7 (3.6)a,b |
Ng 1 | 59.8 (0.2)c | 5.1 (0.1)b | 1.5 (0.2) b,c | 5.3 (0.2)b | 3.0 (0.1) | 129.4 (1.0)a |
Ng 2 | 60.3 (0.3)b,c | 5.5 (0.1)b | 1.7 (0.1) b | 5.2 (0.3)b | 2.8 (0.1) | 118.1 (4.7)b |
Ng 3 | 60.7 (0.1)b | 5.4 (0.3)b | 1.2 (0.3) c | 5.0 (0.2)b | 2.7 (0.2) | 118.7 (6.0)b |
Composite | ||||||
One-way ANOVA, P value | <0.001 | <0.001 | <0.001 | <0.001 | 0.447 | <0.001 |
Control MPS | 64.6 (0.4)a | 10.9 (0.4)a | 2.2 (0.1)a | 4.3 (0.2)a | 6.3 (0.3) | 145.7 (8.7)a |
MPS + Ng 1 | 60.4 (0.4)b,c | 8.7 (0.2)b,c | 1.7 (0.1)b | 3.4 (0.1)b | 6.2 (0.2) | 141.5 (10.6)a |
MPS + Ng 2 | 60.2 (0.8)c | 8.2 (0.3)c | 1.7 (0.1)b | 3.3 (0.1)b | 6.2 (0.1) | 132.2 (3.9)a,b |
MPS + Ng 3 | 60.3 (1.5)c | 7.8 (0.1)c | 1.8 (0.1)b | 3.1 (0.1)b | 6.0 (0.1) | 126.2 (6.2)a,b,c |
VIN Ng 1 | 62.6 (1.1)a,b | 9.9 (0.6)a,b | 1.7 (0.1)b | 4.1 (0.2)a | 6.0 (0.1) | 107.6 (14.2)b,c |
VIN Ng 2 | 60.9 (0.3)b,c | 9.7 (0.2)a,b | 1.7 (0.1)b | 4.2 (0.3)a | 6.4 (0.4) | 108.4 (15.2)b,c |
VIN Ng 3 | 60.3 (0.9)c | 9.2 (0.4)b,c | 1.4 (0.1)c | 4.0 (0.1)a | 6.3 (0.3) | 112.0 (9.1)b,c |
VIN Ng 1 + Ng 1 | 57.3 (0.5)d | 5.4 (0.3)d | 1.1 (0.1)d | 3.1 (0.1)b | 6.1 (0.2) | 102.8 (2.2)c |
VIN Ng 2 + Ng 2 | 56.7 (0.3)d | 6.7 (1.0)d | 1.2 (0.1)d | 3.1 (0.2)b | 6.2 (0.2) | 95.8 (6.5)c |
VIN Ng 3 + Ng 3 | 61.0 (0.1)b,c | 7.8 (0.5)c | 1.2 (0.1)d | 3.0 (0.2)b | 6.2 (0.2) | 94.1 (8.6)c |
Within a column, means followed by the same letter are not statistically different (P > 0.05). Data presented here for DC and RPmax were obtained from polymerization kinetics testing.
ANOVA, analysis of variance; DC, degree of conversion; FM, flexural modulus; FS, flexural strength; MPS, γ-methacryloxypropyltrimethoxysilane; Ng, nanogel; PS, polymerization stress; RPmax, maximum polymerization rate; VIN, trimethoxyvinylsilane; VS, volumetric shrinkage.