Table 4.
1H and 13C nuclear magnetic resonance (NMR) chemical shifts (δ, ppm).
| Sugar residue | H-1 |
H-2 |
H-3 |
H-4 |
H-5 |
H-6 |
|---|---|---|---|---|---|---|
| C-1 | C-2 | C-3 | C-4 | C-5 | C-6 | |
| →6)-duD-Galp-(1→ (A) | 5.14 | 3.69 | 3.74 | 3.91 | 3.95 | 3.73/3.89 |
| 99.8 | 69.5 | 70.4 | 70.0 | 71.5 | 68.1 | |
| →6)-/3D-Glcp-(1→ (B) | 5.08 | 3.35 | 3.59 | 3.41 | 3.73 | 3.88/3.98 |
| 99.8 | 72.7 | 74.1 | 70.4 | 72.3 | 69.3 | |
| →4)-β-D-ManpNAc3NAcA-(1→(C) | 4.99 | 4.30 | 4.29 | 3.94 | 3.88 | |
| 101.3 | 52.9 | 54.5 | 79.7 | 72.9 | 175.9 | |
| →4)-β-D-ManpNAc3NAcA-(1→ (D) | 4.89 | 4.41 | 4.32 | 3.96 | 3.90 | |
| 101.1 | 52.6 | 54.3 | 79.6 | 73.0 | 176.0 | |
| →4)-β-D-GalpNAc-(1→ (E) | 4.64 | 3.97 | 3.85 | 4.14 | 3.73 | 3.76 |
| 102.7 | 52.0 | 82.3 | 68.2 | 76.2 | 62.5 |