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. 2019 Jun 5;24(11):2133. doi: 10.3390/molecules24112133

Table 1.

The considered solvents for the preparation of extracts from different parts of the walnut tree and its fruit.

No Solvent Part References
1 Water Fruit Kernel [28,69,70,136,137,138,139]
Shell [56], [140]25, [141]25
Husk [18,56,73,103,142,143]
Other parts Leaf [78]25, [109], [144]24, [145,146], [147]25, [148,149], [150]28
Bark [128], [151]32, [152,153]
Stem [148]
2 Ethanol Fruit Kernel [28]9, [137], [154]16, [155]11, [156]11, [157]4, [158]34
Skin [154]16, [159]35
Shell [24]4, [140,141], [158]34
Husk [18], [103]4, [142], [158]34, [160]6, [161], [162]4
Other parts Leaf [104]30, [110]6, [145], [149], [158]34, [162]4, [163]31, [164]22, [165]23, [166]22, [167]26, [168,169], [170]20, [171,172], [173]6
Bark [128,151], [174]2
Stem [158]34
Root [21]
3 Methanol Fruit Kernel [27,66,67,131,132,133,134,135,138], [154]17, [175], [176]12, [177], [178]12, [179]14, [180]15, [181]12, [182]
Skin [66,67], [154]16
Shell [56,67,140,141,183]
Husk [18,56,67,71], [103]5, [131,182], [184,185],
Other parts Leaf [77,112,131,145,146,148,165,185,186], [187]27, [188,189,190,191], [192]21, [193,194]
Shoot [80], [81]37, [82]37
Bark [124,151,152,195,196], [197]33, [198]3
Stem [148]
Root [129]
4 Ethyl acetate Fruit Kernel [70]
Shell [56,140,141]
Husk [18,56,142]
Other parts Leaf [165]
Bark [124,152,195]
Root [129]
5 Acetone Fruit Kernel [16]18, [25]10, [46]18, [138], [199]8, [200]13, [201]7, [202]19,
Shell [183]
Husk [18], [102]7, [203]7
Other parts Leaf [145,204]
Bark [124]1, [151], [152]1, [153], [195]8
6 Hexane Fruit Husk [18]
Other parts Leaf [165], [205]29
Bark [196]
Root [129]
7 Dichloromethane Fruit Shell [56]
Husk [56]
8 Petroleum ether Fruit Kernel [70,131]
Husk [131,142]
Other parts Leaf [131]
Bark [151]
9 Chloroform Fruit Shell [140,141]
Husk [142]
Other parts Leaf [79,165]
Bark [151,196]
10 n-Butanol Fruit Kernel [68,70]
Shell [140,141]
11 Benzene Other parts Leaf [145]
Bark [151]
12 Cyclohexane Other parts Leaf [171]

1 in diluted form; 2 80% (400 mL ethanol 96% + 100 mL water); 3 70% aqueous acetone; 4 50% aqueous ethanol; 5 50% aqueous methanol; 6 70% ethanol; 7 acetone/water (v/v, 70/30); 8 acetone:water (80:20; v/v); 9 96%; 10 chilled 80% acetone (1:8, w/w); 11 ethanol:water (4:1, v/v); 12 methanol:water (70:30); 13 acetone:water (60:40; v/v); 14 80% methanol (1:2 w/v, 3×); 15 methanol/water (60:40, v/v); 16 ethanol/water (7:3, v/v); 17 methanol/water (6:4, v/v); 18 75% acetone + 25% of 526 µmol/L sodium metabisulfite; 19 100 mM acetate buffer, pH 4.8/acetone (30:70, v/v); 20 hydroethanolic (20 to 70% v/v); 21 80% methanol (v/v); 22 80% ethanol; 23 ethanol:water (80:20); 24 acidified water (pH 2 with HCl); 25 boiling water; 26 60% ethanol; 27 60% methanol; 28 20% water (w/w) and choline chloride with butyric or phenylpropionic acid (mole ratio 1:2); 29 95% hexane; 30 61% ethanol; 31 ethanol:water (4:6); 32 distilled water; 33 99.5% methanol; 34 95% ethanol (v/v); 35 ethanol:water (4:6); 36 50 or 70% ethanol; 37 80% methanol.