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. Author manuscript; available in PMC: 2019 Dec 7.
Published in final edited form as: ACS Catal. 2018 Nov 1;8(12):11704–11715. doi: 10.1021/acscatal.8b03051

Figure 3.

Figure 3.

EPR data (red) and simulations (black) of ~1 mM Tm FDPNO. (B) WT FDPNo and (C-E) FDPNO of H90 residue variants as listed. Principal components of the S = ½ g tensors are indicated. (A) Simulations of the individual species giving B: WT (solid line), radical impurity (long dash), free NO (short dash). Red arrow for H90D indicates a shoulder matching the H90A species. Conditions: temperature, 6 K; microwaves, 0.2 mW at 9.646 GHz. Simulations (black traces) use the parameters listed in Table 1.