Table 3. Data-collection and refinement statistics for human aquaporin 2 crystallized on Roadrunner II chips.
PDB code | 6qf5 |
Data-collection temperature (K) | 298 |
No. of hits | 3377 |
Indexed patterns | 2903 |
Space group | P42 |
a, b, c (Å) | 122.2, 122.2, 94.14 |
α, β, γ (°) | 90, 90, 90 |
Resolution range (Å) | 37.38–3.70 (3.76–3.70) |
R split | 0.437 (1.538) |
Mean I/σ(I) | 2.32 (0.92) |
Completeness (%) | 99.97 (99.93) |
No. of unique reflections | 14866 (1462) |
Multiplicity | 28.1 (17.7) |
CC* | 0.937 (0.435) |
Wilson B factor (Å2) | 93.37 |
Resolution for refinement | 33.89–3.70 (3.82–3.70) |
No. of reflections used | 14805 (1110) |
No. of reflections used for R free | 1488 (127) |
R work/R free | 0.282/0.336 (0.398/0.419) |
R.m.s.d., bond lengths (Å) | 0.004 |
R.m.s.d., bond angles (°) | 0.761 |
Mean B factor (Å2) | 105.45 |