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. 2019 Jun 21;6(Pt 4):507–520. doi: 10.1107/S2052252519007061

Table 1. Sample-chamber parameters for various pressure ranges.

These parameters are designed for the condition of using a pair of wide-perforated Boehler anvils, together with a methanol:ethanol 4:1 mixture as the pressure medium. Pressure is expected to be increased only at low temperature (typically no higher than 25 K) using a helium diaphragm, in order to reduce the thermal expansion of the pressure medium and any thermal weakening of the gasket strength. The pressure is calibrated by the equation of state for silver (Ag) at T = 4 K using two parameters (bulk modulus B = 108.85 GPa, and B′ = dB/dP = 5.7).

Diamond culet size (µm) Gasket materials Initial shim thickness (µm) Pre-indented thickness (µm) Hole diameter (µm) Targeted pressure (GPa)
800 Stainless Steel 301 305 162 390 18
700 Rhenium 255 156 330 25
600 Rhenium 255 141 280 35
550 Rhenium 255 121 240 42