Table 1.
Data collection and refinement statistics
| GGTase3-FBXL2-SKP1 (PDB 6O60)a | |
|---|---|
| Data collection | |
| Space group | P212121 |
| Cell dimensions | |
| a, b, c (Å) | 86.8, 99.3, 151.2 |
| α, β, γ (°) | 90.0, 90.0, 90.0 |
| Resolution (Å) | 50.00–2.50 (2.54–2.50)b |
| Rmerge | 0.098 (0.890) |
| Rmeas | 0.109 (0.986) |
| I/σ(I) | 24.3 (2.3) |
| CC1/2 | 0.991 (0.754) |
| Completeness (%) | 90.5 (93.6) |
| Redundancy | 4.8 (4.7) |
| Refinement | |
| Resolution (Å) | 49.5–2.5 |
| No. reflections | 41320 |
| Rwork / Rfree | 0.194/0.247 |
| No. atoms | 9299 |
| Protein | 9228 |
| Znion | 1 |
| Water | 70 |
| B factors | |
| Protein | 55 |
| Znion | 41 |
| Water | 51 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.008 |
| Bond angles (°) | 1.025 |
a
A single crystal was used for diffraction data collection and structure determination.
b
Values in parentheses are for highest-resolution shell.