Table 4. Identification by mass spectrometry of O-glycans released from human platelet GPIbα.
RT (min)a | Massb | m/zc | Volume | % Total | Compositiond |
---|---|---|---|---|---|
13.818 | 676.259 | 677.264 | 55954 | 0.1 | 1-1-0-1 |
15.621 | 896.351 | 897.355 | 66130 | 0.2 | 2-2-1-0 |
21.22 | 1041.385 | 1042.393 | 1109306 | 2.9 | 2-2-0-1 |
21.423 | 1058.403 | 1059.408 | 34603 | 0.1 | 3-2-1-0 |
22.534 | 1042.406 | 1043.414 | 86869 | 0.2 | 2-2-2-0 |
24.62 | 896.34 | 897.357 | 34603 | 0.1 | 3-2-1-0 |
24.641 | 1187.442 | 594.729 | 995826 | 2.6 | 2-2-1-1 |
24.894 | 1041.386 | 1042.393 | 892163 | 2.3 | 2-2-0-1 |
24.913 | 750.287 | 751.296 | 321269 | 0.8 | 2-2-0-0 |
28.375 | 1332.473 | 667.248 | 202429 | 0.5 | 2-2-0-2 |
29.585 | 1332.482 | 667.249 | 33180240 | 86.0 | 2-2-0-2 |
31.03 | 1697.612 | 849.818 | 112008 | 0.3 | 3-3-0-2 |
32.243 | 1332.49 | 667.253 | 224937 | 0.6 | 2-2-0-2 |
34.9 | 1697.618 | 849.815 | 1199390 | 3.1 | 3-3-0-2 |
34.904 | 1041.396 | 1042.402 | 66130 | 0.2 | 2-2-0-1 |
aRetention time
bDaltons
cPrecursor ion mass to charge ratio
dHex-HexNAc-Fuc-NeuAc