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. Author manuscript; available in PMC: 2020 Apr 10.
Published in final edited form as: J Am Chem Soc. 2019 Mar 29;141(14):5942–5960. doi: 10.1021/jacs.9b00795

Figure 5.

Figure 5.

80 K, zero applied magnetic field 57Fe Mössbauer spectra (blue) with corresponding fits (orange) at 2 mM in 1:9 MeTHF:toluene: (top) F8Cmpd-II and (bottom) (DCHIm)-F8Cmpd-II. The fits for these Mössbauer spectra indicated a single quadrupole doublet, implying high purity of the samples. Mössbauer parameters are given in Table 1.