Table 3.
Position | 1H NMR δ (ppm) | m, J (Hz) | 13C NMR δ (ppm) |
---|---|---|---|
1 | 1.35–2.34 | M | 35.6 |
2 | 1.35–2.34 | M | 27.8 |
3 | 3.24 | dd, 4.7 and 11.5 | 79.0 |
4 | - | - | 38.6 |
5 | 1.35–2.34 | M | 50.4 |
6 | 1.35–2.34 | M | 18.2 |
7 | 1.35–2.34 | M | 28.2 |
8 and 9 | - | - | 134.4 |
10 | - | - | 37.0 |
11 | 1.35–2.34 | M | 21.0 |
12 | 1.35–2.34 | M | 26.5 |
13 | - | - | 44.5 |
14 | - | - | 49.8 |
15 | 1.35–2.34 | M | 31.3 |
16 | 1.35–2.34 | M | 31.0 |
17 | 1.35–2.34 | M | 50.4 |
18 | 0.70 | S | 15.7 |
19 | 0.99 | S | 18.7 |
20 | 1.35–2.34 | M | 36.5 |
21 | 0.93 | d, 6,4 | 19.1 |
22 | 1.35–2.34 | M | 35.0 |
23 | 1.35–2.34 | M | 30.8 |
24 | - | - | 156.9 |
25 | 2.24 | M | 22.0 |
26 | 1.04 | d, 6.9 | 33.8 |
27 | 1.03 | d, 6.9 | 21.9 |
28 | 4.67 and 4.72 | d and s, 1.2 | 105.9 |
29 | 0.82 | S | 15.4 |
30 | 1.01 | S | 27.9 |
31 | 0.89 | S | 24.3 |
OH | 5.35 | m |