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. 2019 Jun 17;9(6):235. doi: 10.3390/biom9060235

Table 2.

Chemical Shifts of the Disaccharides on AFGP8.

Disaccharide (a) AFGP8 from Boreogadus saida
HN HNAc H1 H2 H3 H4 H5 H6 C1 C2 C3 C4 C5 C6 CNAc
α3 7.18 1.83 4.88 4.18 3.64 3.90 3.71 3.47 98.5 47.8 77.8 67.7 71.2 60.4 22.8
α6 7.06 1.87 4.73 4.13 3.59 3.90 3.68 3.46 98.5 47.8 78.3 67.7 71.2 60.4 22.8
α9 7.15 1.83 4.88 4.13 3.61 3.90 3.71 3.47 98.5 47.8 78.2 67.7 71.2 60.4 22.8
α12 7.34 1.85 4.79 4.14 3.65 3.90 3.68 3.46 98.5 47.8 77.8 67.7 71.2 60.4 22.8
β3 - - 4.24 3.31 3.27 3.62 3.34 3.53 104.1 70.7 72.8 67.9 75.1 60.4 -
β6 - - 4.19 3.32 3.27 3.62 3.34 3.47 104.1 70.7 72.8 67.9 75.1 60.4 -
β9 - - 4.21 3.32 3.27 3.62 3.34 3.53 104.1 70.7 72.8 67.9 75.1 60.4 -
β12 - - 4.29 3.30 3.27 3.62 3.34 3.47 104.1 70.7 72.8 67.9 75.1 60.4 -
Disaccharide (b) AFGP8 from Pathogenia (Trematomus) borchgrevinki
HN HNAc H1 H2 H3 H4 H5 H6 C1 C2 C3 C4 C5 C6 CNAc
α3 7.05 1.87 4.72 4.15 3.62 3.90 3.68 3.47 98.5 47.9 78.2 67.7 71.3 60.4 22.8
α6 7.15 1.84 4.88 4.13 3.61 3.90 3.72 3.48 98.5 48.0 78.2 67.7 71.3 60.4 22.8
α9 7.07 1.87 4.72 4.14 3.58 3.90 3.68 3.47 98.5 47.9 78.3 67.7 71.3 60.4 22.8
α12 7.35 1.81 4.91 4.11 3.64 3.90 3.72 3.48 98.5 48.0 77.9 67.7 71.3 60.4 22.8
β3 - - 4.23 3.28 3.27 3.62 3.34 3.47 104.0 70.6 72.8 67.9 75.1 60.4 -
β6 - - 4.21 3.28 3.27 3.62 3.34 3.53 104.0 70.6 72.8 67.9 75.1 60.4 -
β9 - - 4.20 3.28 3.27 3.62 3.34 3.57 104.0 70.6 72.8 67.9 75.1 60.4 -
β12 - - 4.27 3.30 3.30 3.62 3.34 3.53 104.0 70.6 72.8 67.9 75.1 60.4 -