Table 2.
Position | δC, Type | δH (J in Hz) | COSY | HMBC |
---|---|---|---|---|
2 | 152.6, C | - | ||
3 | 101.0, CH | 6.47, brs | CH3-9 | C-2,4,8 |
4 | 134.7, C | |||
5 | 109.3, CH | 6.70, s | H2-10 | C-6,7,8a,10 |
6 | 154.4, C | - | ||
7 | 95.6, CH | 6.70, s | C-6,8a | |
8 | 155.0, C | - | ||
8a | 118.4, C | - | ||
9 | 13.7, CH3 | 2.36, d (1.0) | C-2,3 | |
10 | 61.0, CH2 | 4.58, d (5.6) | H-5, OH-6 | C-4,5,8a |
OH-6 | - | 9.28, s | C-5,6,7 | |
OH-10 | - | 5.17, t (5.6) | H2-10 | C-10 |