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. 2019 Jun 25;17(6):379. doi: 10.3390/md17060379

Table 2.

1H and 13C NMR (DMSO-d6, 300.13 and 75.4 MHz) and HMBC assignment for 2.

Position δC, Type δH (J in Hz) COSY HMBC
2 152.6, C -
3 101.0, CH 6.47, brs CH3-9 C-2,4,8
4 134.7, C
5 109.3, CH 6.70, s H2-10 C-6,7,8a,10
6 154.4, C -
7 95.6, CH 6.70, s C-6,8a
8 155.0, C -
8a 118.4, C -
9 13.7, CH3 2.36, d (1.0) C-2,3
10 61.0, CH2 4.58, d (5.6) H-5, OH-6 C-4,5,8a
OH-6 - 9.28, s C-5,6,7
OH-10 - 5.17, t (5.6) H2-10 C-10