Scheme 2.
Synthesis route of PCBMA-SS-PCL-SS-PCBMA. (i) CDI, anhydrous DCM, RT., 24 h; (ii) DMSO, pyridine, TEA, RT, 48 h; (iii) DCC, NHS, RT., 48 h; (iv) AIBN, THF, saturated saltwater, 60 °C, 48 h.
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