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. 2019 Jul 1;15:1448–1459. doi: 10.3762/bjoc.15.145

Table 4.

Complexation efficacy of ≈20 mg insoluble CDPs in 0.050 mM MO solution after 1 day and 2 weeks (entry numbers are identical as those in Table 3.)

No. CD used in CDP synthesis Milling time [h] Particle sizea [µm] MO binding capacity [µmol/mg] Relative MO binding capacityb

1 day 14 days

9 β 6 ≈1.9 0.004 0.006 0.33
10e β 9 ≈2.9 0.005 0.009 0.51
11 β*H2O 6 ≈1.7 0.007 0.010 0.61
12 γ 6 ≈1.8 0.003 0.004 0.25
13 γ*H2O 6 ≈2.2 <0.001 0.002 0.10
14 bead polymerc N/A ≈77d 0.011 0.017 1.00

aBy QELS; bbead polymer = 1, calculated with not rounded values; cCyclolab’s CYL-2011; dby electron microscope.