Table 1. Crystallographic data collection and refinement statistics.
| PDB ID Code | 6MW4 |
|---|---|
| Space Group | C222(1) |
| Cell a, b, c (Å) | 88.6, 155.2, 91.7 |
| Resolution Å | 50–1.55 |
| 1(High resolution Å) | (1.61–1.55) |
| Reflections | 91876 |
| Completeness % | 99.9 (99.9) |
| Multiplicity | 6.5 (6.0) |
| Wilson B | 18.1 |
| I/SigmaI | 24.2 (1.7) |
| Rmeas % | 6.6 (17.8) |
| Rpim % | 2.6 (28.8) |
| CC 1/2 | 0.996 (0.857) |
| Coordinate error Å | 0.18 |
| Phase error(˚) | 18.1 |
| Rwork % | 16.4 |
| 2Rfree % | 18.6 |
| Rms bonds Å | 0.006 |
| Rms angles(˚) | 0.806 |
| Ramachandran | |
| Favored | 98.7 |
| Disallowed | 0.37 |
| Mean B Å2 | |
| Protein (atoms) | 27.1 (4214) |
| Solvent (atoms) | 36.9 (375) |
| Sulfate (atoms) | 56.4 (25) |
1Numbers in parentheses denote high resolution.
2Represents 10% of reflections omitted from refinement.