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. Author manuscript; available in PMC: 2020 May 22.
Published in final edited form as: J Am Chem Soc. 2019 May 14;141(20):8116–8127. doi: 10.1021/jacs.8b12082

Figure 10.

Figure 10.

(top) X-Band HYSCORE spectrum of ArP3BFe(NNSiMe3), with comparison (bottom) of experimental data to simulations (grey) of 14Nα (red), 14Nβ (blue) and 11B (green), using the simulation parameters in Table 3. Acquisition parameters: temperature = 20 K; magnetic field = 334.0 mT; microwave frequency = 9.392 GHz; MW pulse length (π/2, π) = 8 ns, 16 ns; τ = 140 ns; t1 = t2 = 100 ns; Δt1 = Δt2 = 16 ns; shot repetition time (srt) = 1 ms).