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. 2017 Feb 10;2(2):487–495. doi: 10.1021/acsomega.7b00028

Table 1. Effect of Additivesa.

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    yield (%)b
entry additive 2a 3
1 LiBr 0 72 (67)c
2 78 (70)c 0
3 LiCl 0 13
4d n-Bu4NBr 0 34
5e n-Bu4NCl 0 50
6 n-Bu4NHSO4 0 13
7 NaBr 0 26
8 KBr 0 23
9 LiBF4 41 0
a

All reactions were conducted with 0.194 mmol of 1 in DME (1.0 mL).

b

Determined by 1H NMR analysis using an internal standard.

c

Isolated yield is given in parentheses.

d

Ynone 1 was recovered in 29% yield.

e

Ynone 1 was recovered in 25% yield.