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. 2017 Feb 10;2(2):487–495. doi: 10.1021/acsomega.7b00028

Table 2. Screening of the Reaction Conditions for the Cascade Wacker/Allylation Sequencea.

graphic file with name ao-2017-000285_0004.jpg

entry Pd Cu atmosphere yield (%)b
1 + + Ar 70
2 + O2 56
3 + Ar 69
4 + O2 0
5 + Ar 0
6 O2 0
7 Ar 0
a

All reactions were conducted with 0.194 mmol of 1 in DME (1.0 mL).

b

Determined by 1H NMR analysis using an internal standard.