Table 4. Molar Ratio of the Components in the Synthesis of Hierarchically Structured Spinels and the Respective Sample Names.
Ni + Al or Co + Al | EtOH | H2O | PO | PEO contenta (MW 900 000) (mol %) | Ni or Co contentb (mol %) | Ni–Al or Co–Al molar ratio | sample name |
---|---|---|---|---|---|---|---|
1 | 5.4 | 18.1 | 3.1 | 2.8 × 10–6 | 3 | 0.03 | 3Ni-1, 3Co-1 |
3.5 × 10–6 | 3Ni-2, 3Co-2 | ||||||
2.8 × 10–6 | 22 | 0.28 | 22Ni-1, 22Co-1 | ||||
3.5 × 10–6 | 22Ni-2, 22Co-2 | ||||||
2.8 × 10–6 | 33 | 0.50 | 33Ni-1, 33Co-1 | ||||
3.5 × 10–6 | 33Ni-2, 33Co-2 |
Based on the total amount of Ni or Co + Al + PEO.
Based on total amount of metal (Ni or Co + Al).