Table 4. Cu-Catalyzed Coupling and Cyclization of 4 with 2 Leading to 5a.
Reaction conditions: 4 (0.3 mmol), 6 (0.6 mmol) CuI (0.06 mmol), K2CO3 (0.9 mmol), DMF (3 mL), 130 °C, 1 h, under microwave irradiation (100 W of initial power).
Reaction conditions: 4 (0.3 mmol), 6 (0.6 mmol) CuI (0.06 mmol), K2CO3 (0.9 mmol), DMF (3 mL), 130 °C, 1 h, under microwave irradiation (100 W of initial power).