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Conditions A: substrate (1 mmol), Fe(NO3)3·9H2O (0.05 mmol), TEMPO (0.05 mmol), 50 °C, AcOH (2 mL), and oxygen balloon. Conditions B: substrate (1 mmol), Fe(NO3)3·9H2O (0.05 mmol, 20 mg), TEMPO (0.05 mmol), NaNO2 (0.05 mmol, 3.4 mg), CH3CN (5 mL), 50 °C, 10 h, and oxygen balloon.
Conversions and yields are based on gas chromatography (GC) with area normalization. NR = no reaction. Conv. = conversion.
