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(a) Experimental static VT 13C SSNMR spectra of 13CO2-loaded α-Zn3(HCOO)6 recorded from 123 to 433 K at 9.4 T, and (b) the corresponding analytical simulations. Asterisk (*) denotes the unbound CO2 resonance. The spectra simulated from 273 to 433 K are given as summations (dotted black trace) of the adsorbed (solid blue trace) and free (solid red trace) CO2 signals. The 13C CS tensor parameters obtained from the analytical simulations are provided in Table S10.
