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. 2019 Feb 22;4(2):4000–4011. doi: 10.1021/acsomega.8b03623

Figure 7.

Figure 7

(a) Experimental static VT 13C SSNMR spectra of 13CO in α-Zn3(HCOO)6 obtained from 173 to 433 K (Bo = 9.4 T), and (b) the corresponding analytical simulations. Free CO resonances are marked with asterisks (*). The analytical simulations acquired from 193 to 433 K are given as summation spectra (dotted black trace) constructed from the free (solid red trace) and adsorbed (solid blue trace) CO resonances. The 13C CS tensor parameters obtained from the simulations can be found in Table S11.