Table 4. Effect of the Amount of Dried NaI Used in the Synthesis of the Highly Steric Compound 42.
amount of NaI (equiv) | conversiona (%) |
---|---|
0 | 19 |
0.1 | 74 |
0.2 | 66 |
0.5 | 25 |
50 °C, 24 h.
amount of NaI (equiv) | conversiona (%) |
---|---|
0 | 19 |
0.1 | 74 |
0.2 | 66 |
0.5 | 25 |
50 °C, 24 h.